4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

Base Information

Chemical Name:4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide
CAS No.:82146-20-1
Molecular Formula:C₂₉H₃₅O₄P
Molecular Weight:478.568
Hs Code.:

Synonyms:4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

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Chemical Property of 4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

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Technology Process of 4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

There total 3 articles about 4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34573-99-4
4,8-bis(1,1-dimethylethyl)-2,10-dimethyl-6-phenoxy-12H-dibenzo<1.3.2>dioxaphosphocin

: 617-94-7
1-methyl-1-phenylethyl alcohol

: 82146-20-1
4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

Guidance literature:: With Cumene hydroperoxide; In chlorobenzene; at 30 ℃; Kinetics; Mechanism; Thermodynamic data; E_A = 77 kJ/mol, ΔS(excit) = -42 J/Kmol;

Reference yield:

: 34573-99-4
4,8-bis(1,1-dimethylethyl)-2,10-dimethyl-6-phenoxy-12H-dibenzo<1.3.2>dioxaphosphocin

: 82146-20-1
4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

Guidance literature:: With Cumene hydroperoxide; In benzene; at 20 ℃; Rate constant;

Reference yield:

: 119460-24-1
phenyl (2,2'-methylenebis-4-methyl-6-tert-butylphenyl) phosphite ozonide

: 82146-20-1
4,8-Di-tert-butyl-2,10-dimethyl-6-phenoxy-12H-5,7-dioxa-6-phospha-dibenzo[a,d]cyclooctene 6-oxide

Guidance literature:: In dichloromethane; at -1 ℃; Rate constant; Thermodynamic data; various solvents (CHCl3, CCl4, PhCl, CH3NO2, MeCN etc.); decomposition of phosphite ozonides, lg A₀, E_o-ΔG₀^<*>, ΔS^<*>, effect of the structure of ozonide and solvent on rate constant;
DOI:10.1007/BF01455468