2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

Base Information

Chemical Name:2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen
CAS No.:123476-45-9
Molecular Formula:C₂₃H₁₈O₂
Molecular Weight:326.395
Hs Code.:

Synonyms:2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

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Chemical Property of 2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

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Technology Process of 2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

There total 3 articles about 2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1,2-Bis(2-methoxy-5-methylphenyl)-3-phenylcyclopropenyliumtetrafluoroborat

: 123476-45-9
2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

Guidance literature:: With boron tribromide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1055/s-1989-27254

Reference yield:

: 24648-07-5
2-Phenyl-1,3,3-trichlorocyclopropene

: 123476-45-9
2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

Guidance literature:: Multi-step reaction with 2 steps

2: 41 percent / BBr₃ / CH₂Cl₂ / 4 h / 20 °C

With boron tribromide; In dichloromethane;
DOI:10.1055/s-1989-27254

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 123476-45-9
2-(2-Hydroxy-5-methylphenyl)-3-(3-methyl-6-oxo-2,4-cyclohexadienyliden)-1-phenylcyclopropen

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) AlCl₃ / 1.) CH₂Cl₂, 20 deg C, 15 min, 2.) 0 deg C, 2 h

3: 41 percent / BBr₃ / CH₂Cl₂ / 4 h / 20 °C

With aluminium trichloride; boron tribromide; In dichloromethane;
DOI:10.1055/s-1989-27254