(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

Base Information

Chemical Name:(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane
CAS No.:1309314-60-0
Molecular Formula:C₂₅H₂₃N₃OS
Molecular Weight:413.543
Hs Code.:

Synonyms:(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

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Chemical Property of (6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

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Technology Process of (6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

There total 3 articles about (6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 620988-03-6
diisopropyl 2-([tetrahydro-2H-pyran-2-yl]thio)phenylboronate

: 1309314-59-7
(6-bromopyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

: 1309314-60-0
(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

Guidance literature:: diisopropyl 2-([tetrahydro-2H-pyran-2-yl]thio)phenylboronate; (6-bromopyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane; With potassium fluoride; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; for 5h; Reflux;

With acetic acid; In tetrahydrofuran; water; at 50 ℃; for 2h;

Reference yield:

: 1309314-58-6
(6-bromopyridin-2-yl)bis(6-methylpyridin-2-yl)methanol

: 1309314-60-0
(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 40 °C

1.2: 20 h / 20 °C

2.1: potassium fluoride / palladium diacetate; tri-tert-butyl phosphine / tetrahydrofuran / 5 h / Reflux

2.2: 2 h / 50 °C

With potassium fluoride; sodium hydride; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 99765-49-8
bis(6-methylpyridin-2-yl)methanone

: 1309314-60-0
(6-(phenyl-2-thiol)pyridin-2-yl)bis(6-methylpyridin-2-yl)methoxymethane

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / diethyl ether / -78 °C

1.3: 0 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 40 °C

2.2: 20 h / 20 °C

3.1: potassium fluoride / palladium diacetate; tri-tert-butyl phosphine / tetrahydrofuran / 5 h / Reflux

3.2: 2 h / 50 °C

With potassium fluoride; n-butyllithium; sodium hydride; tri-tert-butyl phosphine; palladium diacetate; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;