3-nitro-pyrene-1,6-dione

Base Information

• Chemical Name: 3-nitro-pyrene-1,6-dione
• CAS No.: 858267-50-2
• Molecular Formula: C₁₆H₇NO₄
• Molecular Weight: 277.236
• Mol file: 858267-50-2.mol

Synonyms:3-nitro-pyrene-1,6-dione

Chemical Property of 3-nitro-pyrene-1,6-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3-nitro-pyrene-1,6-dione

There total 8 articles about 3-nitro-pyrene-1,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyrene (129-00-0) → 3-nitro-pyrene-1,6-dione (858267-50-2)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous H₂SO₄; K₂cr2O₇

2: acetic acid; nitric acid

With potassium dichromate; sulfuric acid; nitric acid; acetic acid;

Reference yield:

1,3,6,8-tetrachloropyrene (81-29-8) → 3-nitro-pyrene-1,6-dione (858267-50-2)

Guidance literature:

Multi-step reaction with 5 steps

1: chlorine; trichlorobenzene / 100 °C

2: ethanolic alkaline solution / Behandeln des erhaltenen Gemisches von 1.3.4.6.8.9-Hexachlor-pyren und 1.3.4.6.8.10-Hexachlor-pyren mit Salpetersaeure (D: 1,5) unterhalb 20grad

3: aqueous NaOH; nickel catalyst / 130 °C / 36775.4 Torr / Hydrogenation

4: aqueous NaOH; aqueous NaOCl solution

5: acetic acid; nitric acid

With sodium hydroxide; sodium hypochlorite; alkaline solution; nitric acid; chlorine; nickel; acetic acid; 1,2,3-trichlorobenzene;

Reference yield:

1,3,6,8-tetranitropyrene (28767-61-5) → 3-nitro-pyrene-1,6-dione (858267-50-2)

Guidance literature:

Multi-step reaction with 6 steps

1: PCl₅; trichlorobenzene

2: chlorine; trichlorobenzene / 100 °C

3: ethanolic alkaline solution / Behandeln des erhaltenen Gemisches von 1.3.4.6.8.9-Hexachlor-pyren und 1.3.4.6.8.10-Hexachlor-pyren mit Salpetersaeure (D: 1,5) unterhalb 20grad

4: aqueous NaOH; nickel catalyst / 130 °C / 36775.4 Torr / Hydrogenation

5: aqueous NaOH; aqueous NaOCl solution

6: acetic acid; nitric acid

With sodium hydroxide; sodium hypochlorite; alkaline solution; phosphorus pentachloride; nitric acid; chlorine; nickel; acetic acid; 1,2,3-trichlorobenzene;

upstream raw materials:

pyrene-1,6-dione

pyrene

1,3,6,8-tetrachloropyrene

1,3,6,8-tetranitropyrene

Downstream raw materials:

naphthalene-1,4,5,8-tetracarboxylic acid