C₂₄H₃₀O₆

Base Information

Chemical Name:C₂₄H₃₀O₆
CAS No.:1365268-38-7
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

C<sub>24</sub>H<sub>30</sub>O<sub>6</sub>

Synonyms:C₂₄H₃₀O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₀O₆

Chemical Property:

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Technology Process of C₂₄H₃₀O₆

There total 17 articles about C₂₄H₃₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₆

: 18107-18-1
diazomethyl-trimethyl-silane

: 1365268-38-7
C₂₄H₃₀O₆

Guidance literature:: With methanol; In benzene; at 20 ℃;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: 1365268-46-7
C₄₀H₅₄O₅Si

: 1365268-38-7
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

3.2: -78 °C

4.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

5.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

6.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

7.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

8.1: hydrogenchloride; water / tetrahydrofuran / 45 °C

9.1: Dess-Martin periodane / dichloromethane / 20 °C

10.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

11.1: methanol / benzene / 20 °C

With hydrogenchloride; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; pig liver esterase; 2-methyl-but-2-ene; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; tert-butyl alcohol; benzene; 9.1: Dess-Martin oxidation / 10.1: Pinnick oxidation;
DOI:10.1016/j.tetlet.2012.01.058

Reference yield:

: C₁₉H₂₄O₂

: 1365268-38-7
C₂₄H₃₀O₆

Guidance literature:: Multi-step reaction with 17 steps

1.1: toluene-4-sulfonic acid / benzene / Reflux

2.1: n-butyllithium / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 20 °C

3.2: 0 °C

3.3: -78 °C

4.1: 1H-imidazole / dichloromethane / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / 60 °C

6.1: diisobutylaluminium hydride / dichloromethane / -78 °C

7.1: hydrogenchloride; water / tetrahydrofuran / 20 °C

8.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

9.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C

9.2: -78 °C

10.1: N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 50 °C

11.1: pyridine hydrofluoride / tetrahydrofuran / 0 °C

12.1: pig liver esterase; water / dimethyl sulfoxide / 17 h / 30 °C / pH 8 / aq. phosphate buffer; Enzymatic reaction

13.1: dmap; 2-methyl-6-nitrobenzoic anhydride / dichloromethane / 20 °C / High dilution conditions

14.1: hydrogenchloride; water / tetrahydrofuran / 45 °C

15.1: Dess-Martin periodane / dichloromethane / 20 °C

16.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 20 °C

17.1: methanol / benzene / 20 °C

With 1H-imidazole; hydrogenchloride; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; pig liver esterase; 2-methyl-but-2-ene; pyridine hydrofluoride; 2-methyl-6-nitrobenzoic anhydride; water; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; tert-butyl alcohol; benzene; 15.1: Dess-Martin oxidation / 16.1: Pinnick oxidation;
DOI:10.1016/j.tetlet.2012.01.058