Technology Process of C18H25N3O4S
There total 7 articles about C18H25N3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C12H15N3O2S; dimethyl sulfate;
In
acetonitrile;
at 50 ℃;
for 2h;
di-tert-butyl dicarbonate;
With
triethylamine;
In
acetonitrile;
at 20 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium hydride / diethyl ether; dimethyl sulfoxide; mineral oil / 3.58 h / 20 - 35 °C
2.1: water; sulfuric acid / 8 h / Reflux
3.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
3.2: 3 h / 100 °C
4.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
5.1: acetone / 1 h / 20 °C
6.1: sodium hydroxide; water / methanol / 0.17 h / 50 °C
7.1: acetonitrile / 2 h / 50 °C
7.2: 2.5 h / 20 °C
With
sulfuric acid; diphenyl phosphoryl azide; water; sodium hydride; triethylamine; sodium hydroxide; lithium hydroxide;
In
methanol; diethyl ether; dimethyl sulfoxide; acetone; toluene; acetonitrile; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
1.2: 3 h / 100 °C
2.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
3.1: acetone / 1 h / 20 °C
4.1: sodium hydroxide; water / methanol / 0.17 h / 50 °C
5.1: acetonitrile / 2 h / 50 °C
5.2: 2.5 h / 20 °C
With
diphenyl phosphoryl azide; water; triethylamine; sodium hydroxide; lithium hydroxide;
In
methanol; dimethyl sulfoxide; acetone; toluene; acetonitrile;
