7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Base Information

Chemical Name:7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran
CAS No.:105631-21-8
Molecular Formula:C₂₀H₃₀O
Molecular Weight:286.458
Hs Code.:

Synonyms:7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Suppliers and Price of 7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

There total 5 articles about 7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 110418-50-3
C₂₀H₂₉ClHgO

: 105631-21-8
7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Guidance literature:: With sodium hydroxide; sodium tetrahydroborate; In ethanol; dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1021/jo00231a011

Reference yield:

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 105631-21-8
7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / HMPA

2: 61 percent / Li / liquid ammonia / 0.17 h / -78 °C

3: 1.) Hg(OSO₂CF₃)2*C₆H₅N(CH₃)2, 2.) NaBH₄ / 1.) nitromethane, dichloromethane, -20 grad C, 2 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; Hg(OSO₂CF₃)2*C₆H₅N(CH₃)2; lithium; In ammonia;
DOI:10.1016/S0040-4039(00)83973-8

Reference yield:

: 105631-15-0
13-(p-toluenesulfonyl)ambliofuran

: 105631-21-8
7-Methyl-7-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-4,5,6,7-tetrahydro-benzofuran

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / Li / liquid ammonia / 0.17 h / -78 °C

2: 1.) Hg(OSO₂CF₃)2*C₆H₅N(CH₃)2, 2.) NaBH₄ / 1.) nitromethane, dichloromethane, -20 grad C, 2 h

With sodium tetrahydroborate; Hg(OSO₂CF₃)2*C₆H₅N(CH₃)2; lithium; In ammonia;
DOI:10.1016/S0040-4039(00)83973-8