6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile

Base Information

• Chemical Name: 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile
• CAS No.: 1012330-26-5
• Molecular Formula: C₂₈H₃₇N₃O₂Si
• Molecular Weight: 475.706

Synonyms:6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile

Chemical Property of 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile

Chemical Property:

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Technology Process of 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile

There total 1 articles about 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-[(tert-butyldimethylsilyl)oxy]-1-(5-tributylstannyloxazol-2-yl)-7-phenylheptane + 6-bromopyridin-2-carbonitrile (122918-25-6) → 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile (1012330-26-5)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 16h; Heating;

DOI:10.1021/jm701210y

Reference yield: 92.0%

6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinonitrile (1012330-26-5) → 6-(2-(1-hydroxy-7-phenylheptyl)oxazol-5-yl)picolinonitrile (1012330-27-6)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1021/jm701210y

upstream raw materials:

6-bromopyridin-2-carbonitrile

Downstream raw materials:

6-(2-(1-hydroxy-7-phenylheptyl)oxazol-5-yl)picolinonitrile

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