Technology Process of C17H21N3O4
There total 7 articles about C17H21N3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; p-toluenesulfonyl chloride;
In
dichloromethane;
at 20 ℃;
for 16h;
DOI:10.1021/jm3014376
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - -40 °C
1.2: 16 h / -78 - -40 °C
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 45 °C
3.1: dichloromethane / 16 h / 20 °C
4.1: tetrahydrofuran / 16 h / 50 °C
5.1: p-toluenesulfonyl chloride; triethylamine / dichloromethane / 16 h / 20 °C
With
tetrabutyl ammonium fluoride; potassium hexamethylsilazane; triethylamine; p-toluenesulfonyl chloride;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jm3014376
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 16 h / 20 °C
2: tetrahydrofuran / 16 h / 50 °C
3: p-toluenesulfonyl chloride; triethylamine / dichloromethane / 16 h / 20 °C
With
triethylamine; p-toluenesulfonyl chloride;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm3014376