triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

Base Information

Chemical Name:triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate
CAS No.:85289-43-6
Molecular Formula:BF₄*C₂₀H₂₆B₁₀P
Molecular Weight:492.315
Hs Code.:

Synonyms:triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

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Chemical Property of triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

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Technology Process of triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

There total 2 articles about triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 99506-47-5
phenyl(m-carboran-9-yl)chloronium tetrafluoroborate

: 17819-85-1
9-chloro-m-carborane

: 85289-43-6
triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

: 426-79-9
tetraphenylphosphonium tetrafluoroborate

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: With triphenylphosphine; In acetone; Irradiation (UV/VIS); irradiated for 38 h, 56°C; treated with ether, soln. reduced, treated with methyl iodide, refluxed for 1.5 h, extracted with hexane, filtered, GLC, (31)P-NMR;

Reference yield: 82.0%

: 84633-96-5
bis-9-M-carboranylbromonium borofluoride

: 17819-81-7
9-bromo(1,7-dicarba-closo-dodecaborane⁽¹²⁾)

: 85289-43-6
triphenyl(m-carboran-9-yl)phosphonium tetrafluoroborate

Guidance literature:: With triphenylphosphine; In acetone; Irradiation (UV/VIS); a soln. of fluoroborate salt and P(C6H5)3 irradiated for 20 h; concentrated; treated with ether; pptd.; reprecipitated with ether fromacetone and from CHCl3; elem. anal.;
DOI:10.1007/BF00957970