C₃₁H₄₁ClO₇Si

Base Information

Chemical Name:C₃₁H₄₁ClO₇Si
CAS No.:1332271-28-9
Molecular Formula:C₃₁H₄₁ClO₇Si
Molecular Weight:589.201
Hs Code.:

C<sub>31</sub>H<sub>41</sub>ClO<sub>7</sub>Si

Synonyms:C₃₁H₄₁ClO₇Si

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Chemical Property of C₃₁H₄₁ClO₇Si

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Technology Process of C₃₁H₄₁ClO₇Si

There total 6 articles about C₃₁H₄₁ClO₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1332271-27-8
C₃₂H₄₀ClF₃O₁₀SSi

: 1332271-65-4
C₃₁H₄₁ClO₇Si

: 1332271-28-9
C₃₁H₄₁ClO₇Si

Guidance literature:: With chromium dichloride; nickel dichloride; In N,N-dimethyl-formamide; at 20 ℃; for 1h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: C₃₁H₄₅ClO₇Si

: 1332271-28-9
C₃₁H₄₁ClO₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 °C / Inert atmosphere

4.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

5.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: chromium dichloride; nickel dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With pyridine; chromium dichloride; tetrapropylammonium perruthennate; sulfur trioxide pyridine complex; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; pyridine hydrogenfluoride; dimethyl sulfoxide; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; nickel dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 6.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1016/j.tet.2011.04.094

Reference yield:

: 1332271-63-2
C₃₁H₄₃ClO₇Si

: 1332271-28-9
C₃₁H₄₁ClO₇Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 40 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 1.17 h / -78 °C / Inert atmosphere

2.2: 0.5 h / -78 °C / Inert atmosphere

3.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere

4.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 4 h / 20 °C / Inert atmosphere; Molecular sieve

5.1: chromium dichloride; nickel dichloride / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

With pyridine; chromium dichloride; tetrapropylammonium perruthennate; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; nickel dichloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; 5.1: Nozaki-Hiyama-Kishi reaction;
DOI:10.1016/j.tet.2011.04.094