methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

Base Information

Chemical Name:methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate
CAS No.:73184-98-2
Molecular Formula:C₂₁H₂₄ClFO₃
Molecular Weight:378.871
Hs Code.:

Synonyms:methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

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Technology Process of methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

There total 3 articles about methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 59606-93-8
<(2,5-dimethyl-4-methoxy-6-chlorophenyl)methyl>triphenylphosphonium chloride

: 69877-78-7
methyl (2E,4E,6Z)-3-methyl-6-fluoro-7-formyl-2,4,6-octatrienoate

: 73184-98-2
methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

Guidance literature:: With ethyloxirane; In toluene; at 80 - 90 ℃; for 15h;
DOI:10.1021/jm00343a014

Reference yield:

: 62924-29-2
(E)-4-Dimethylphosphono-3-methyl-2-butenoate

: 73184-98-2
methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 5 deg C, 2 h, 2.) DMF, 5 deg C, 2 h

2: 80 percent / 1,2-epoxybutane / toluene / 15 h / 80 - 90 °C

With ethyloxirane; sodium hydride; In toluene;
DOI:10.1021/jm00343a014

Reference yield:

: 200860-79-3
4,4-dimethoxy-2-fluoro-3-methyl-2-buten-1-al

: 73184-98-2
methyl (2E,4E,6Z,8E)-3,7-dimethyl-6-fluoro-9-(2,5-dimethyl-4-methoxy-6-chlorophenyl)-2,4,6,8-nonatetraenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 5 deg C, 2 h, 2.) DMF, 5 deg C, 2 h

2: 80 percent / 1,2-epoxybutane / toluene / 15 h / 80 - 90 °C

With ethyloxirane; sodium hydride; In toluene;
DOI:10.1021/jm00343a014