4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

Base Information

Chemical Name:4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole
CAS No.:1443247-12-8
Molecular Formula:C₉₆H₁₃₀O₄S₃₂
Molecular Weight:2374.2
Hs Code.:

4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

Synonyms:4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

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Chemical Property of 4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

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Technology Process of 4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

There total 1 articles about 4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1443247-11-7
{[4-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}(triisopropyl)silane

: 1443247-12-8
4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; water; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/chem.201102868

Reference yield: 45.0%

: 1443247-12-8
4-({2-[2-{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-5-ethynyl-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

: 1443247-05-9
4,4'-[(2-iodo-1,4-phenylene)bis(oxyethane-2,1-diylthio)]bis[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole]

: 1443247-03-7
4-({2-[2,5-bis{[2,5-bis(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenyl]ethynyl}-4-(2-{[4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiol-4-yl]thio}ethoxy)phenoxy]ethyl}thio)-4',5,5'-tris(butylthio)-2,2'-bi-1,3-dithiole

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 72h; Inert atmosphere;
DOI:10.1002/chem.201102868