(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

Base Information

Chemical Name:(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)
CAS No.:117939-43-2
Molecular Formula:C₃₉H₃₁FeO₆PSi
Molecular Weight:710.578
Hs Code.:

(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh<sub>3</sub>)

Synonyms:(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

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Chemical Property of (OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

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Technology Process of (OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

There total 2 articles about (OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 117958-59-5
trans-{Fe(CO)3{P(OPh)3}SiPh₃}Et₄N

: 117939-43-2
(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

Guidance literature:: With HCl; In diethyl ether; under N2; suspension of complex in ether treated at room temp. with 0.13N HCl in ether; concd.; addn. of hexane; crystn. at -20°C;

Reference yield: 76.0%

: 101-02-0
triphenyl phosphite

: 30351-80-5
cis-Fe(CO)4(H)Si(C₆H₅)3

: 18475-06-4,49655-15-4
tetracarbonylirontriphenylphosphite

: 15526-65-5,20516-74-9
trans-tricarbonylbis(triphenylphosphite)iron

: 117939-43-2
(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

Guidance literature:: In hexane; byproducts: Ph3SiH, CO; under N2 in hexane at room temp.; filtered; recrystn. (1/1 CH2Cl2/hexane); elem. anal.;

Reference yield: 92.0%

: 117939-43-2
(OC-6-23)-Fe(CO)3{P(OPh)3}(H)(SiPh₃)

: 117958-59-5
trans-{Fe(CO)3{P(OPh)3}SiPh₃}Et₄N

Guidance literature:: With NaH; (C₂H₅)4NCl; In tetrahydrofuran; dichloromethane; byproducts: NaCl; under N2; addn. of complex soln. to suspension of NaH in THF at room temp.; after 30 min evapn.; residue taken up in CH2Cl2; treated with Et4NCl soln.; solid formed; evapn.; washed (water); dissolved (CH2Cl2); dried (MgSO4); carefully addn. of hexane (two layers); crystn. at -20°C; elem. anal.;