Technology Process of Al(3-(4-formamidophenyl)pentane-2,4-dionate)3
There total 1 articles about Al(3-(4-formamidophenyl)pentane-2,4-dionate)3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
NaHCO3;
In
methanol; water;
addn. of aq. soln. of aluminium compd. to methanolic soln. diketone deriv. with stirring, addn. of aq. soln. of NaHCO3; isolation of ppt., triturating with water and methanol, drying in air, elem. anal.;
DOI:10.1021/ic900202e
- Guidance literature:
-
With
POCl3; NH(CH(CH3)2)2;
In
dichloromethane;
addn. of POCl3 to CH2Cl2 soln. of aluminium compd. and amine deriv. at room temp. under Ar, stirring for 1 h; washing with aq. NaHCO3, concg., addn. of hexane, isolation of ppt., drying at 70°C, elem. anal.;
DOI:10.1021/ic900202e
- Guidance literature:
-
Multi-step reaction with 2 steps
1: POCl3; NH(CH(CH3)2)2 / dichloromethane
2: dichloromethane
With
POCl3; NH(CH(CH3)2)2;
In
dichloromethane;
DOI:10.1021/ic900202e
