Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

Base Information

Chemical Name:Al(3-(4-formamidophenyl)pentane-2,4-dionate)3
CAS No.:1194041-75-2
Molecular Formula:C₃₆H₃₆AlN₃O₉
Molecular Weight:681.678
Hs Code.:

Synonyms:Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

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Chemical Property of Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

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Technology Process of Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

There total 1 articles about Al(3-(4-formamidophenyl)pentane-2,4-dionate)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: aluminum(III) nitrate nonahydrate

: 1194041-73-0
3-(4-formamidophenyl)pentane-2,4-dione

: 1194041-75-2
Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

Guidance literature:: With NaHCO₃; In methanol; water; addn. of aq. soln. of aluminium compd. to methanolic soln. diketone deriv. with stirring, addn. of aq. soln. of NaHCO3; isolation of ppt., triturating with water and methanol, drying in air, elem. anal.;
DOI:10.1021/ic900202e

Reference yield: 75.0%

: 1194041-75-2
Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

: 1194041-79-6
Al(3-(4-isocyanophenyl)pentane-2,4-dionate)3

Guidance literature:: With POCl₃; NH(CH(CH₃)2)2; In dichloromethane; addn. of POCl3 to CH2Cl2 soln. of aluminium compd. and amine deriv. at room temp. under Ar, stirring for 1 h; washing with aq. NaHCO3, concg., addn. of hexane, isolation of ppt., drying at 70°C, elem. anal.;
DOI:10.1021/ic900202e

Reference yield:

: 1194041-75-2
Al(3-(4-formamidophenyl)pentane-2,4-dionate)3

: 1194041-82-1
Al(3-(4-isocyanophenyl)pentane-2,4-dionate)3(AuCl)3

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃; NH(CH(CH₃)2)2 / dichloromethane

2: dichloromethane

With POCl₃; NH(CH(CH₃)2)2; In dichloromethane;
DOI:10.1021/ic900202e