C₂₆H₂₈N₂O₂

Base Information

Chemical Name:C₂₆H₂₈N₂O₂
CAS No.:1448446-88-5
Molecular Formula:C₂₆H₂₈N₂O₂
Molecular Weight:400.521
Hs Code.:

C<sub>26</sub>H<sub>28</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₆H₂₈N₂O₂

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Chemical Property of C₂₆H₂₈N₂O₂

Chemical Property:

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Technology Process of C₂₆H₂₈N₂O₂

There total 9 articles about C₂₆H₂₈N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1448446-92-1
C₂₈H₃₂N₂O₃

: 1448446-88-5
C₂₆H₂₈N₂O₂

Guidance literature:: With hydrogenchloride; In ethanol; water; for 3h; Reflux;
DOI:10.1002/anie.201206734

Reference yield:

: 19716-82-6
1-(phenylmethyl)-3-ethyl-1,4,5,6-tetrahydropyridine

: 1448446-88-5
C₂₆H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: dichloromethane / 24 h / 20 °C

2.1: zinc-copper couple / diethyl ether / 18 h / 0 - 20 °C / Sonication

3.1: ammonium chloride / methanol / 3 h / Reflux

4.1: toluene-4-sulfonic acid / benzene / 13 h / Dean-Stark; Reflux

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 °C

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / 20 °C

7.2: 2.5 h

8.1: hydrogenchloride / water; ethanol / 3 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/anie.201206734

Reference yield:

: 1246190-33-9
3,4-dihydro-2H-5-ethylpyridine-1-carboxylic acid benzyl ester

: 1448446-88-5
C₂₆H₂₈N₂O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: zinc-copper couple / diethyl ether / 18 h / 0 - 20 °C / Sonication

2.1: ammonium chloride / methanol / 3 h / Reflux

3.1: toluene-4-sulfonic acid / benzene / 13 h / Dean-Stark; Reflux

4.1: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 °C

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.67 h / 20 °C

6.2: 2.5 h

7.1: hydrogenchloride / water; ethanol / 3 h / Reflux

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium hydride; ammonium chloride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; benzene;
DOI:10.1002/anie.201206734