Technology Process of C28H32N2O5
There total 7 articles about C28H32N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; tetrabutylammonium perrhenate;
In
dichloromethane;
at 20 ℃;
for 11h;
DOI:10.1021/jo060084f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 91 percent / (TMS)3SiH; AIBN / toluene / 100 °C
2.1: 91 percent / DMAP; triethylamine / CH2Cl2 / 1 h / 20 °C
3.1: n-BuLi / tetrahydrofuran; hexane / -78 - 0 °C
3.2: 96 percent / tetrahydrofuran; hexane / 0.58 h / -78 °C
4.1: 100 percent / tetrabutylammonium perrhenate; p-toluenesulfonic acid / CH2Cl2 / 11 h / 20 °C
With
dmap; n-butyllithium; 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane; toluene-4-sulfonic acid; triethylamine; tetrabutylammonium perrhenate;
In
tetrahydrofuran; hexane; dichloromethane; toluene;
4.1: Meyer-Schuster rearrangement;
DOI:10.1021/jo060084f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran; hexane / -78 - 0 °C
1.2: 96 percent / tetrahydrofuran; hexane / 0.58 h / -78 °C
2.1: 100 percent / tetrabutylammonium perrhenate; p-toluenesulfonic acid / CH2Cl2 / 11 h / 20 °C
With
n-butyllithium; toluene-4-sulfonic acid; tetrabutylammonium perrhenate;
In
tetrahydrofuran; hexane; dichloromethane;
2.1: Meyer-Schuster rearrangement;
DOI:10.1021/jo060084f
