2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

Base Information

Chemical Name:2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide
CAS No.:131653-66-2
Molecular Formula:C₂₃H₃₁N₃O₂
Molecular Weight:381.518
Hs Code.:

Synonyms:2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

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Chemical Property of 2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

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Technology Process of 2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

There total 3 articles about 2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 113975-32-9
2,2-dimethyl-N-(4-iodo-3-pyridinyl)propanamide

: 103681-98-7
2-diisopropylaminocarbonylphenylboronic acid

: 131653-66-2
2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 12h; Heating;

Reference yield:

: 70298-88-3
N-(pyridin-3-yl)pivalamide

: 131653-66-2
2-[3-(2,2-dimethylpropanoylamino)pyridin-4-yl]-N,N-diisopropylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi, 2) I₂ / 1) Et₂O, -10 deg C, 2) -70 to -10 deg C

2: 85 percent / 2M aq. NaHCO₃ / Pd(PPh₃)4 / toluene / 12 h / Heating

With n-butyllithium; iodine; sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;