C₅₇H₁₀₀O₉Si₄

Base Information

Chemical Name:C₅₇H₁₀₀O₉Si₄
CAS No.:213824-35-2
Molecular Formula:C₅₇H₁₀₀O₉Si₄
Molecular Weight:1041.76
Hs Code.:

C<sub>57</sub>H<sub>100</sub>O<sub>9</sub>Si<sub>4</sub>

Synonyms:C₅₇H₁₀₀O₉Si₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₇H₁₀₀O₉Si₄

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Technology Process of C₅₇H₁₀₀O₉Si₄

There total 19 articles about C₅₇H₁₀₀O₉Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₇H₁₀₂O₉Si₄

: 213824-35-2
C₅₇H₁₀₀O₉Si₄

Guidance literature:: With pyridine; sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1002/anie.199725201

Reference yield:

: 201142-54-3
(Z)-2-[(2S,3S,4S,5R)-4,5-Bis-(tert-butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-tetrahydro-pyran-2-yloxymethyl]-3-[(1S,2R,6R)-6-isopropyl-3-methyl-2-((2S,3S)-3-methyl-2,3-bis-triethylsilanyloxy-pent-4-ynyl)-cyclohex-3-enyl]-propenal

: 213824-35-2
C₅₇H₁₀₀O₉Si₄

Guidance literature:: Multi-step reaction with 2 steps

1: LiHMDS / tetrahydrofuran / 0.17 h / -30 °C

2: NaHCO₃, pyridine, Dess-Martin reagent / CH₂Cl₂ / 0.25 h / 0 °C

With pyridine; sodium hydrogencarbonate; Dess-Martin periodane; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja9810639

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 213824-35-2
C₅₇H₁₀₀O₉Si₄

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / Et₃N / CH₂Cl₂ / 2 h / 0 °C

2: 80 percent / NBS, pyridine / acetone; H₂O

3: 93 percent / NaH / CH₂Cl₂ / 3.5 h / 25 °C

4: TMSOTf / hexane / -78 °C

5: LiHMDS / tetrahydrofuran / 0.17 h / -30 °C

6: NaHCO₃, pyridine, Dess-Martin reagent / CH₂Cl₂ / 0.25 h / 0 °C

With pyridine; N-Bromosuccinimide; trimethylsilyl trifluoromethanesulfonate; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; water; acetone;
DOI:10.1021/ja9810639