benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

Base Information

Chemical Name:benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate
CAS No.:1354053-50-1
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:

Synonyms:benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

Chemical Property:

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Technology Process of benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

There total 4 articles about benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 3459-92-5
DBC

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 1354053-50-1
benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

Guidance literature:: With potassium carbonate; In 1,2-dimethoxyethane; for 12h; chemoselective reaction; Reflux;
DOI:10.1039/c1gc15796e

Reference yield:

: 3459-92-5
DBC

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 1354053-50-1
benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

: 15028-56-5
4-(benzyloxymethyl)-2,2-dimethyl-1,3-dioxolane

Guidance literature:: With potassium carbonate; at 190 ℃; for 18h; chemoselective reaction; Autoclave; Inert atmosphere;
DOI:10.1039/c1gc15796e

Reference yield:

: 13326-10-8
benzyl methyl carbonate

: 1354053-50-1
benzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrotalcite KW₂₀₀₀ / 4 h / 110 °C

2: potassium carbonate / 18 h / 190 °C / Autoclave; Inert atmosphere

With potassium carbonate;
DOI:10.1039/c1gc15796e