C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide

Base Information

• Chemical Name: C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide
• CAS No.: 634178-99-7
• Molecular Formula: C₁₇H₁₉N₃O₅S
• Molecular Weight: 377.421

Synonyms:C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide

Chemical Property of C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide

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Technology Process of C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide

There total 2 articles about C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C33H31N3O7S (634178-95-3) → C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide (634178-99-7)

Guidance literature:

With sodium methylate; In methanol;

DOI:10.1039/c0cc00645a

Reference yield: 97.0%

→ C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide (634178-99-7)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 16h;

DOI:10.1016/S0968-0896(03)00229-3

Reference yield: 81.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazol-4-yl)phenyl]carboxamide (634178-99-7) → (2R,4S,5R)-5-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-hydroxy-tetrahydro-furan-2-carboxylic acid [3-(2-acetylamino-thiazol-4-yl)-phenyl]-amide

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 4h;

DOI:10.1016/S0968-0896(03)00229-3

upstream raw materials:

C₃₃H₃₁N₃O₇S

Downstream raw materials:

5'-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

5'-(N-α,δ,ω-tri-Z-L-arginyl)-C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

3',5'-di-(N-α,δ,ω-tri-Z-L-arginyl)-C-(2'-deoxy-β-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

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