(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

Base Information

Chemical Name:(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine
CAS No.:1017581-25-7
Molecular Formula:C₃₅H₄₆O₄Si₂
Molecular Weight:586.919
Hs Code.:

Synonyms:(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

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Technology Process of (Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

There total 1 articles about (Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1017581-24-6
(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-hydroxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

: 15933-59-2
1,1,3,3-tetramethyldisilazane

: 1017581-25-7
(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

Guidance literature:: With ammonium chloride; at 60 ℃;
DOI:10.1039/b715354f

Reference yield: 61.0%

: 1017581-25-7
(Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine

: 1017581-26-8
(Z,2R,3S,8S,9R)-8-benzyloxy-9-tbutyldiphenylsilyoxymethyl-3-hydroxy-2-hydroxymethyl-2,3,4,7,8,9-hexahydro-oxonine

Guidance literature:: (Z,3S,8S,9R)-benzyloxy-9-tbutyldiphenylsilyloxymethyl-3-dimethylsilyloxy-2-methylene-4,7,8,9-tetrahydro-3H-oxonine; (bicyclo(2.2.1)hepta-2,5-diene)(1,4-(Ph₂P)2butane)Rh(I) BF₄; In acetone; for 18h; Heating;

With potassium hydroxide; dihydrogen peroxide; In tetrahydrofuran; methanol; for 1h; Further stages.;
DOI:10.1039/b715354f