11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

Base Information

Chemical Name:11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine
CAS No.:105576-42-9
Molecular Formula:C₁₅H₁₂N₈
Molecular Weight:304.314
Hs Code.:

Synonyms:11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

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Chemical Property of 11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

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Technology Process of 11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

There total 4 articles about 11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 105576-45-2
6-Benzylidenehydrazino-9,9-dimethyl-9H-pyrazolo<3,4-d>-s-triazolo<4,3-b>pyridazine

: 105576-42-9
11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

Guidance literature:: With bromine; sodium acetate; In acetic acid; for 3h; Ambient temperature;
DOI:10.1055/s-1986-31486

Reference yield:

: 94794-93-1
6-chloro-9,9-dimethyl-9H-pyrazolo<4,3-d>-1,2,4-triazolo<4,3-b>pyridazine

: 105576-42-9
11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 80percent hydrazine hydrate / ethanol / 3 h / Heating

2: 90 percent / methanol / 5 h / Heating

3: 85 percent / Br₂, NaOAc / acetic acid / 3 h / Ambient temperature

With bromine; sodium acetate; hydrazine hydrate; In methanol; ethanol; acetic acid;
DOI:10.1055/s-1986-31486

Reference yield:

: 105576-44-1
9,9-Dimethyl-6-hydrazino-9H-pyrazolo<4,3-d>-s-triazolo<4,3-b>pyridazine

: 105576-42-9
11,11-Dimethyl-6-phenyl-11H-pyrazolo<3,4-d>-bis-s-triazolo<4,3-b:3',4'-f>pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / methanol / 5 h / Heating

2: 85 percent / Br₂, NaOAc / acetic acid / 3 h / Ambient temperature

With bromine; sodium acetate; In methanol; acetic acid;
DOI:10.1055/s-1986-31486