N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

Base Information

Chemical Name:N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine
CAS No.:1194488-53-3
Molecular Formula:C₁₅H₂₃NOS
Molecular Weight:265.42
Hs Code.:

Synonyms:N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

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Chemical Property of N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

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Technology Process of N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

There total 6 articles about N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₁NOS

: 1194488-53-3
N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

Guidance literature:: C₁₅H₂₁NOS; With sodium tetrahydroborate; In methanol; at 20 ℃; for 16h;

With hydrogenchloride; water; In methanol;

Reference yield:

: 929000-14-6
methyl 5-bromo-2-(methylthio)benzoate

: 1194488-53-3
N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

Guidance literature:: Multi-step reaction with 6 steps

1.1: 9-borabicyclo-[3.3.1]nonane dimer / tetrahydrofuran / 20 °C

1.2: 16 h / 80 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

4.1: formic acid; magnesium sulfate / dichloromethane / 20 °C

5.1: formic acid; magnesium sulfate / dichloromethane / 20 °C

6.1: sodium tetrahydroborate / methanol / 16 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; formic acid; 9-borabicyclo-[3.3.1]nonane dimer; sodium hydrogencarbonate; magnesium sulfate; Dess-Martin periodane; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1229245-25-3
5-[3-(methyloxy)propyl]-2-(methylthio)benzaldehyde

: 1194488-53-3
N-{[5-[3-(methyloxy)propyl]-2-(methylthio)phenyl]methyl}cyclopropan amine

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid; magnesium sulfate / dichloromethane / 20 °C

2: formic acid; magnesium sulfate / dichloromethane / 20 °C

3: sodium tetrahydroborate / methanol / 16 h / 20 °C

With sodium tetrahydroborate; formic acid; magnesium sulfate; In methanol; dichloromethane;