10:2 FTOH Sulfate PotassiuM Salt

Base Information

• Chemical Name: 10:2 FTOH Sulfate PotassiuM Salt
• CAS No.: 1262446-14-9
• Molecular Formula: C₁₂H₄F₂₁O₄S*K
• Molecular Weight: 682.292
• Mol file: 1262446-14-9.mol

Synonyms:potassium 12,12,12,11,11,10,10,9,9,8,8,7,7,6,6,5,5,4,4,3,3-heneicosafluorododecyl sulfate

Chemical Property of 10:2 FTOH Sulfate PotassiuM Salt

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Mono[2-(perfluorodecyl)ethyl]SulfatePotassiumSalt ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Mono[2-(perfluorodecyl)ethyl] Sulfate is the sulfate conjugate of 8-2 Fluorotelomer Alcohol, a raw material used in the manufacturing of fluorotelomer-based products.

Technology Process of 10:2 FTOH Sulfate PotassiuM Salt

There total 1 articles about 10:2 FTOH Sulfate PotassiuM Salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.8%

ethyleneglycol sulfate (1072-53-3) + 1-Iodo-perfluorodecane (423-62-1) → potassium 12,12,12,11,11,10,10,9,9,8,8,7,7,6,6,5,5,4,4,3,3-heneicosafluorododecyl sulfate (1262446-14-9)

Guidance literature:

1-Iodo-perfluorodecane; With ethylmagnesium bromide; In diethyl ether; at -78 - -40 ℃; for 0.5h; Inert atmosphere;

ethyleneglycol sulfate; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In diethyl ether; at -78 - -40 ℃; Inert atmosphere;

With water; potassium carbonate; at 50 ℃; for 3h;

DOI:10.1016/j.jfluchem.2010.09.004

Reference yield: 89.0%

potassium 12,12,12,11,11,10,10,9,9,8,8,7,7,6,6,5,5,4,4,3,3-heneicosafluorododecyl sulfate (1262446-14-9) → 2-(perfluorodecyl)ethanol (865-86-1)

Guidance literature:

With hydrogenchloride; water; at 70 ℃; for 25h; pH=0 - 1;

DOI:10.1016/j.jfluchem.2010.09.004

upstream raw materials:

ethyleneglycol sulfate

1-Iodo-perfluorodecane

Downstream raw materials:

2-(perfluorodecyl)ethanol

Refernces