1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside

Base Information

• Chemical Name: 1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside
• CAS No.: 1240486-92-3
• Molecular Formula: C₄₉H₇₀O₁₂
• Molecular Weight: 851.088
• Mol file: 1240486-92-3.mol

Synonyms:1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside

Chemical Property of 1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside

There total 1 articles about 1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C34H38Cl3NO10 (1240486-80-9) + (S)-methyl 11-hydroxyhexadecanoate (121043-05-8) → 1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside (1240486-92-3)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 25 ℃; Molecular sieve; Inert atmosphere;

DOI:10.1021/jo101231r

Reference yield: 91.0%

1-(methoxycarbonyl)pentadec-10(S)-yl 2-O-acetyl-3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside (1240486-92-3) → 1-(methoxycarbonyl)pentadec-10(S)-yl 3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside (1240486-94-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; dichloromethane; at 0 - 40 ℃; Inert atmosphere;

DOI:10.1021/jo101231r

upstream raw materials:

C₃₄H₃₈Cl₃NO₁₀

(S)-methyl 11-hydroxyhexadecanoate

Downstream raw materials:

1-(methoxycarbonyl)pentadec-10(S)-yl 3,4,6-tri-O-p-methoxybenzyl-β-D-glucopyranoside