3-(4-Bromophenyl)-3-(3-pyridyl)allylamine

Base Information

Chemical Name:3-(4-Bromophenyl)-3-(3-pyridyl)allylamine
CAS No.:60324-67-6
Molecular Formula:C₁₄H₁₃BrN₂
Molecular Weight:289.175
Hs Code.:2933399090
Mol file:60324-67-6.mol

Synonyms:3-(4-bromophenyl)-3-(3-pyridyl)allylamine;3-(4-bromophenyl)-3-(3-pyridyl)allylamine ethanedioate, (Z)-isomer;3-(4-bromophenyl)-3-(3-pyridyl)allylamine, (E)-isomer;CPP 200;CPP-200

Suppliers and Price of 3-(4-Bromophenyl)-3-(3-pyridyl)allylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-(4-Bromophenyl)-3-(3-pyridyl)allylamine

Chemical Property:

Vapor Pressure:1.82E-07mmHg at 25°C
Boiling Point:426.1°C at 760 mmHg
Flash Point:211.5°C
PSA：38.91000
Density:1.377g/cm3
LogP:3.93480
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:359.97957
Heavy Atom Count:19
Complexity:257

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CN=C1)C(=CCN)C2=CC=C(C=C2)Br.Cl.Cl
Isomeric SMILES:C1=CC(=CN=C1)/C(=C\CN)/C2=CC=C(C=C2)Br.Cl.Cl

Technology Process of 3-(4-Bromophenyl)-3-(3-pyridyl)allylamine

There total 19 articles about 3-(4-Bromophenyl)-3-(3-pyridyl)allylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82103-82-0
(Z)-1-(4-bromophenyl)-3-pthalimido-1-(3-pyridyl)propene

: 60324-67-6
(Z)-3-(4-bromophenyl)-3-(3-pyridyl)allylamine

Guidance literature:: With hydrazine hydrate; In methanol; at 60 ℃; for 5h;
DOI:10.3891/acta.chem.scand.36b-0091

Reference yield:

: 14548-45-9
(4-bromophenyl)-pyridin-3-yl-methanone

: 60324-67-6
(Z)-3-(4-bromophenyl)-3-(3-pyridyl)allylamine

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 5 h / 60 °C

2: 70 percent / ClCOOCH₂CCl₃ / benzene / 2 h / Heating

3: 41 percent / dimethylformamide / 3 h / 80 °C

4: 1.25 g / H₂NNH₂*H₂O / methanol / 5 h / 60 °C

With hydrazine hydrate; 2,2,2-Trichloroethyl chloroformate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; benzene;
DOI:10.3891/acta.chem.scand.36b-0091

Reference yield:

: 60324-61-0
ethyl 3-(4-bromophenyl)-3-hydroxy-3-(3-pyridyl)propionate

: 60324-67-6
(Z)-3-(4-bromophenyl)-3-(3-pyridyl)allylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 76 percent / LiAlH₄ / diethyl ether / 5 h / Heating

2: PBr₃ / CH₂Cl₂ / Heating

3: H₂O / 4 h / Ambient temperature

4: 70 percent / ClCOOCH₂CCl₃ / benzene / 2 h / Heating

5: 41 percent / dimethylformamide / 3 h / 80 °C

6: 1.25 g / H₂NNH₂*H₂O / methanol / 5 h / 60 °C

With lithium aluminium tetrahydride; phosphorus tribromide; hydrazine hydrate; 2,2,2-Trichloroethyl chloroformate; In methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; benzene;
DOI:10.3891/acta.chem.scand.36b-0091