ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

Base Information

Chemical Name:ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate
CAS No.:1449112-05-3
Molecular Formula:C₂₂H₂₆ClN₃O₃S₃
Molecular Weight:512.118
Hs Code.:

Synonyms:ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

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Chemical Property of ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

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Technology Process of ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

There total 2 articles about ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 882280-82-2
C₁₅H₁₂ClNO₂S₂

: C₇H₁₆N₂O₂S

: 1449112-05-3
ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 6h;
DOI:10.1039/c3md00065f

Reference yield:

: tert-butyl 2-(2-ethoxy-2-oxoethyl)-2-(2-(methylthio)ethyl)hydrazinecarboxylate

: 1449112-05-3
ethyl 2-(2-(3-(4-chlorophenyl)-4-cyano-5-(isopropylthio)thiophene-2-carbonyl)-1-(2-(methylthio)ethyl)hydrazinyl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-methyl-morpholine / dichloromethane / 6 h / 20 °C

With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3md00065f