C₅₉H₇₀N₆O₁₂

Base Information

Chemical Name:C₅₉H₇₀N₆O₁₂
CAS No.:1379654-59-7
Molecular Formula:C₅₉H₇₀N₆O₁₂
Molecular Weight:1055.24
Hs Code.:

C<sub>59</sub>H<sub>70</sub>N<sub>6</sub>O<sub>12</sub>

Synonyms:C₅₉H₇₀N₆O₁₂

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Chemical Property of C₅₉H₇₀N₆O₁₂

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Technology Process of C₅₉H₇₀N₆O₁₂

There total 13 articles about C₅₉H₇₀N₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1379654-58-6
C₆₀H₇₂N₆O₁₂

: 1379654-59-7
C₅₉H₇₀N₆O₁₂

Guidance literature:: C₆₀H₇₂N₆O₁₂; With lithium hydroxide monohydrate; dihydrogen peroxide; In methanol; at 0 ℃; for 1h;

In methanol; at 20 ℃; for 22h;
DOI:10.1002/chem.201103185

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 1379654-59-7
C₅₉H₇₀N₆O₁₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran; toluene / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / dimethyl sulfoxide / 20 h / 80 °C / Inert atmosphere

3.1: sodium periodate; ammonium acetate; water / acetone / 17 h / 20 °C

4.1: lithium hydroxide monohydrate / tetrahydrofuran; methanol / 1 h / 0 °C

4.2: 1 h / 20 °C

5.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C

5.2: 96 h / 20 °C

6.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 2 h / 90 °C

7.1: tetrabutylammonium hydrogen sulfate / dichloromethane / 2 h / 20 °C

8.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

10.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C

10.2: 22 h / 20 °C

With sodium periodate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; lithium hydroxide monohydrate; ammonium acetate; water; dihydrogen peroxide; potassium acetate; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; triphenylphosphine; tetrabutylammonium hydrogen sulfate; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; 6.1: Suzuki coupling;
DOI:10.1002/chem.201103185

Reference yield:

: 691394-91-9
methyl (S)-3-(4-(benzyloxy)-3-iodophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1379654-59-7
C₅₉H₇₀N₆O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane / 1 h / 20 °C

2.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

3.1: 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C

3.2: 96 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / methanol; water; toluene / 2 h / 90 °C

5.1: tetrabutylammonium hydrogen sulfate / dichloromethane / 2 h / 20 °C

6.1: trifluoroacetic acid / chloroform / 1 h / 0 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-hydroxy-3,4-dihydrobenzotriazine-4-one / tetrahydrofuran / 72 h / 0 - 20 °C / Inert atmosphere

8.1: lithium hydroxide monohydrate; dihydrogen peroxide / methanol / 1 h / 0 °C

8.2: 22 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-hydroxy-7-aza-benzotriazole; lithium hydroxide monohydrate; tetrabutylammomium bromide; dihydrogen peroxide; sodium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-hydroxy-3,4-dihydrobenzotriazine-4-one; tetrabutylammonium hydrogen sulfate; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; 4.1: Suzuki coupling;
DOI:10.1002/chem.201103185