4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one

Base Information

• Chemical Name: 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one
• CAS No.: 1220095-33-9
• Molecular Formula: C₂₁H₁₉ClN₆O₂
• Molecular Weight: 422.874

Synonyms:4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one

Chemical Property of 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one

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Technology Process of 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one

There total 5 articles about 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

5-amino-1-(2-chlorobenzyl)-4-cyanoformimidoylimidazole + 4-methoxybenzyl isocyanate (56651-60-6) → 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one (1220095-33-9)

Guidance literature:

5-amino-1-(2-chlorobenzyl)-4-cyanoformimidoylimidazole; 4-methoxybenzyl isocyanate; In acetonitrile; at 0 - 20 ℃; for 6h; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 1h;

DOI:10.1021/ml100281b

Reference yield:

5-amino-1-(2-chlorobenzyl)-4-cyanoformimidoylimidazole + 4-methoxybenzyl isocyanate (56651-60-6) → C21H19ClN6O2 (1261168-08-4) + 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one (1220095-33-9)

Guidance literature:

In acetonitrile; at 0 - 20 ℃; for 6h; Inert atmosphere;

Reference yield:

C21H19ClN6O2 (1261168-08-4) → 4-(1-(2-chlorobenzyl)-5-amino-1H-imidazol-4-yl)-1-(4-methoxybenzyl)-5-imino-1H-imidazol-2(5H)-one (1220095-33-9)

Guidance literature:

1,8-diazabicyclo[5.4.0]undec-7-ene; at 20 ℃; for 1h; Inert atmosphere;

upstream raw materials:

4-methoxybenzyl isocyanate

C₂₁H₁₉ClN₆O₂

N¹-(2-chlorobenzyl)-N²-(Z)-[2-amino-1,2-dicyanovinyl]formamidine

Downstream raw materials:

3,7-dihydro-3-[(4-methoxyphenyl)methyl]-7-[(2-chlorophenyl)methyl]-2H-diimidazo[4,5-d:4',5'-f][1,3]diazepin-2-one

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