6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

Base Information

Chemical Name:6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate
CAS No.:43077-04-9
Molecular Formula:C₂₀H₂₁N₅O₆
Molecular Weight:427.417
Hs Code.:

Synonyms:6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

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Chemical Property of 6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

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Technology Process of 6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

There total 8 articles about 6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.6%

: 43077-03-8
N⁶-benzoyl-5'-deoxy-2',3'-O-isopropylidiene-5',5'-(N,N'-diphenylethylenediamino)adenosine

: 43077-04-9
6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

Guidance literature:: With water; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1021/ml4002503

Reference yield:

: 362-75-4
2',3'-isopropylidene adenosine

: 43077-04-9
6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine

2: NaOH / pyridine

3: DMSO; dicyclohexylcarbodiimide; H⁺

4: Dowex 50 (acid form) / tetrahydrofuran

With pyridine; sodium hydroxide; Dowex 50 (acid form); hydrogen cation; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; pyridine;
DOI:10.1016/j.tetasy.2003.11.007

Reference yield:

: 39947-04-1
N-6-benzoyl-2',3'-O-isopropylideneadenosine

: 43077-04-9
6-N-benzoyl-9-(2,3-O-isopropylidene-β-D-ribo-pentodialdo-1,5-furanosyl)adeninehydrate

Guidance literature:: Multi-step reaction with 2 steps

1: DMSO; dicyclohexylcarbodiimide; H⁺

2: Dowex 50 (acid form) / tetrahydrofuran

With Dowex 50 (acid form); hydrogen cation; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2003.11.007