C₃₅H₃₂ClFN₄O₄

Base Information

Chemical Name:C₃₅H₃₂ClFN₄O₄
CAS No.:1369595-36-7
Molecular Formula:C₃₅H₃₂ClFN₄O₄
Molecular Weight:627.115
Hs Code.:

C<sub>35</sub>H<sub>32</sub>ClFN<sub>4</sub>O<sub>4</sub>

Synonyms:C₃₅H₃₂ClFN₄O₄

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Chemical Property of C₃₅H₃₂ClFN₄O₄

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Technology Process of C₃₅H₃₂ClFN₄O₄

There total 10 articles about C₃₅H₃₂ClFN₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 30186-18-6
4'-bromo-2'-hydroxyacetophenone

: 1369595-36-7
C₃₅H₃₂ClFN₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / ethanol / 15 h / 90 °C

2: polyphosphoric acid / 2 h / 110 °C

3: caesium carbonate / acetonitrile / 15 h / 60 °C

4: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 4 h / 95 °C / Inert atmosphere; Microwave irradiation

5: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

With potassium acetate; sodium carbonate; caesium carbonate; acetic acid; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; ethanol; acetonitrile;

Reference yield:

: 1369594-40-0
C₁₃H₁₈BrN₃O₂

: C₂₈H₂₆BClFNO₄

: 1369595-36-7
C₃₅H₃₂ClFN₄O₄

Guidance literature:: With sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,4-dioxane; at 95 ℃; for 6h; Inert atmosphere;

Reference yield:

: 197142-34-0
(1R,3S,5R)-2-(tert-butoxycarbonyl)-2-azabicyclo[3.1.0]hexane-3-carboxylic acid

: 1369595-36-7
C₃₅H₃₂ClFN₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-THF / tetrahydrofuran / 16.33 h / 0 - 20 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere

2.2: 1.67 h / -78 - 0 °C

3.1: ammonia / methanol / 15.58 h / 20 °C

4.1: N-Bromosuccinimide / tetrahydrofuran / 4.5 h / 20 °C

5.1: ethylenediaminetetraacetic acid; ammonia; zinc / methanol; water / 6 h / 20 °C

6.1: sodium carbonate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 6 h / 95 °C / Inert atmosphere

With N-Bromosuccinimide; borane-THF; oxalyl dichloride; ethylenediaminetetraacetic acid; ammonia; sodium carbonate; dimethyl sulfoxide; zinc; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water;