C₃₅H₄₅N₃O₅

Base Information

Chemical Name:C₃₅H₄₅N₃O₅
CAS No.:1354551-62-4
Molecular Formula:C₃₅H₄₅N₃O₅
Molecular Weight:587.759
Hs Code.:

C<sub>35</sub>H<sub>45</sub>N<sub>3</sub>O<sub>5</sub>

Synonyms:C₃₅H₄₅N₃O₅

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Chemical Property of C₃₅H₄₅N₃O₅

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Technology Process of C₃₅H₄₅N₃O₅

There total 10 articles about C₃₅H₄₅N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1354551-61-3
C₃₅H₄₇N₃O₆

: 1354551-62-4
C₃₅H₄₅N₃O₅

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 872346-84-4
benzyl (3S,4S)-3-hydroxy-4-methyloctanoate

: 1354551-62-4
C₃₅H₄₅N₃O₅

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; diisopropyl-carbodiimide / dichloromethane; water / 30 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

5: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

6: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

7: diethylamino-sulfur trifluoride / dichloromethane / -78 °C / Inert atmosphere

With hydrogenchloride; dmap; 1-hydroxy-7-aza-benzotriazole; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; diisopropyl-carbodiimide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 1354551-64-6
(3S,4S)-3-(Boc-D-Chg-O)-4-methyloctanoic acid

: 1354551-62-4
C₃₅H₄₅N₃O₅

Guidance literature:: Multi-step reaction with 5 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

4: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

5: diethylamino-sulfur trifluoride / dichloromethane / -78 °C / Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.045