3,5-DiiodobenzeneAceticAcid

Base Information

Chemical Name:3,5-DiiodobenzeneAceticAcid
CAS No.:221700-19-2
Molecular Formula:C₈H₆I₂O₂
Molecular Weight:387.943
Hs Code.:
Mol file:221700-19-2.mol

Synonyms:3,5-diiodophenylacetic acid

Suppliers and Price of 3,5-DiiodobenzeneAceticAcid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AK Scientific
2-(3,5-Diiodophenyl)aceticacid
5g
$ 3508.00

AK Scientific
2-(3,5-Diiodophenyl)aceticacid
2.5g
$ 2404.00

AK Scientific
2-(3,5-Diiodophenyl)aceticacid
100mg
$ 506.00

Total 2 raw suppliers

Chemical Property of 3,5-DiiodobenzeneAceticAcid

Chemical Property:

Melting Point:195-196 °C (decomp)
Boiling Point:434.7±40.0 °C(Predicted)
PKA:4.00±0.10(Predicted)
Density:2.409±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

2-(3,5-Diiodophenyl)aceticacid ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-DiiodobenzeneAceticAcid

There total 3 articles about 3,5-DiiodobenzeneAceticAcid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 221700-18-1
ethyl 3,5-diiodophenylacetate

: 221700-19-2
3,5-diiodophenylacetic acid

Guidance literature:: With sodium hydroxide; In water; for 3h; Heating;
DOI:10.1002/1099-0690(200011)2000:22<3771::AID-EJOC3771>3.0.CO;2-1

Reference yield:

: 172607-49-7
4-Amino-3,5-diiodophenylacetic acid

: 221700-19-2
3,5-diiodophenylacetic acid

Guidance literature:: With copper(I) oxide; ethanol; sulfuric acid; Erhitzen des Reaktionsgemisches;
DOI:10.1039/jr9470000202

Reference yield:

: 1197-55-3
4-aminophenylacetic acid

: 221700-19-2
3,5-diiodophenylacetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / ICl; HCl / H₂O / 18 h / 20 °C

2: NaNO₂; H₂SO₄ / 1 h / Heating

3: 95 percent / NaOH / H₂O / 3 h / Heating

With hydrogenchloride; sodium hydroxide; sulfuric acid; Iodine monochloride; sodium nitrite; In water; 1: Iodination / 2: Diazotization / 3: Hydrolysis;
DOI:10.1002/1099-0690(200011)2000:22<3771::AID-EJOC3771>3.0.CO;2-1