C₃₂H₄₂N₂O₃Si

Base Information

Chemical Name:C₃₂H₄₂N₂O₃Si
CAS No.:1269788-53-5
Molecular Formula:C₃₂H₄₂N₂O₃Si
Molecular Weight:530.783
Hs Code.:

C<sub>32</sub>H<sub>42</sub>N<sub>2</sub>O<sub>3</sub>Si

Synonyms:C₃₂H₄₂N₂O₃Si

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Chemical Property of C₃₂H₄₂N₂O₃Si

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Technology Process of C₃₂H₄₂N₂O₃Si

There total 3 articles about C₃₂H₄₂N₂O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₆N₂O₆SSi

: 1269788-53-5
C₃₂H₄₂N₂O₃Si

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 1.5h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: 1269788-45-5
benzyl (R)-3-(tert-butyldimethylsilyloxymethyl)-4-oxopiperidine-1-carboxylate

: 1269788-53-5
C₃₂H₄₂N₂O₃Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1.5 h / -78 °C / Inert atmosphere

2.1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 6 h / 20 °C / Inert atmosphere

3.1: pyridine; dmap / 0.75 h / 0 - 20 °C / Inert atmosphere

4.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere

4.2: 12 h / -65 °C / Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice; Inert atmosphere

6.1: pyridine / 1.5 h / 0 - 20 °C / Inert atmosphere

7.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; n-butyllithium; 20 % Pd(OH)2/C; potassium tert-butylate; hydrogen; diisopropylamine; In tetrahydrofuran; methanol; hexane; ethyl acetate; 1.1: Peterson olefination / 1.2: Peterson olefination;
DOI:10.1016/j.tetlet.2010.12.066

Reference yield:

: 1269788-52-4
C₃₂H₄₂N₂O₄Si

: 1269788-53-5
C₃₂H₄₂N₂O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 2 h / 20 °C / Cooling with ice; Inert atmosphere

2: pyridine / 1.5 h / 0 - 20 °C / Inert atmosphere

3: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With pyridine; sodium tetrahydroborate; potassium tert-butylate; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2010.12.066