C₃₆H₃₃N₉O₇S₄*ClH

Base Information

• Chemical Name: C₃₆H₃₃N₉O₇S₄*ClH
• CAS No.: 1452389-71-7
• Molecular Formula: C₃₆H₃₃N₉O₇S₄*ClH
• Molecular Weight: 868.439

Synonyms:C₃₆H₃₃N₉O₇S₄*ClH

Chemical Property of C₃₆H₃₃N₉O₇S₄*ClH

Chemical Property:

Purity/Quality:

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Technology Process of C₃₆H₃₃N₉O₇S₄*ClH

There total 1 articles about C₃₆H₃₃N₉O₇S₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-chloro-6-methoxypyridine-3-carboxylic acid (503000-87-1) → C36H33N9O7S4*ClH (1452389-71-7)

Guidance literature:

Multi-step reaction with 11 steps

1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / tetrahydrofuran / 3 h / 0 °C

2: Dess-Martin periodane / dichloromethane / 6 h / 20 °C / Inert atmosphere

3: triethylamine; triphenylphosphine; iodine / dichloromethane / 15 h / 0 - 20 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 48 h / 80 °C

5: hydrogen bromide; acetic acid / 28 h / 20 °C

6: triethylamine / dichloromethane / 4 h / 0 °C

7: 2,6-dimethylpyridine; dmap / dichloromethane / 2 h / 0 °C

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl acetamide / 1 h / 45 °C

9: palladium; hydrogen / dichloromethane; ethanol / 3.5 h / 20 °C / 750.08 Torr

10: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 18 h / 0 - 20 °C

11: hydrogenchloride / 1,4-dioxane / 6.5 h / 20 °C

With 2,6-dimethylpyridine; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; hydrogen; iodine; benzotriazol-1-ol; Dess-Martin periodane; palladium; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl acetamide; N,N-dimethyl-formamide; 2: |Dess-Martin Oxidation / 4: |Stille Cross Coupling / 8: |Negishi Coupling;

DOI:10.1002/anie.201302372

upstream raw materials:

2-chloro-6-methoxypyridine-3-carboxylic acid

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