(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

Base Information

Chemical Name:(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide
CAS No.:82783-67-3
Molecular Formula:C₂₉H₄₄O₇SSi
Molecular Weight:564.816
Hs Code.:

(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

Synonyms:(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

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Chemical Property of (1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

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Technology Process of (1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

There total 4 articles about (1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82769-87-7
(1'S,1R,2R,3S,4S,6R)-2,6-dimethyl-3-<(((1'-phenylethyl)amino)carbonyl)oxy>-4-(phenylsulfonyl)cyclohexane-1,2-diol 1,2-acetonide

: 82783-67-3
(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / Heating

2: 1.) KDA / 1.) THF

With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1021/ja00385a030

Reference yield:

: 82769-84-4,82769-85-5
((S)-1-Phenyl-ethyl)-carbamic acid 2,2,3a,7-tetramethyl-5-phenylsulfanyl-hexahydro-benzo[1,3]dioxol-4-yl ester

: 82783-67-3
(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

Guidance literature:: Multi-step reaction with 3 steps

1: 15.0 g / m-chloroperbenzoic acid / CH₂Cl₂ / 1.) -35 deg C, 10 min, 2.) -35 deg C -> 25 deg C, 1 h

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / Heating

3: 1.) KDA / 1.) THF

With Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00385a030

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 82783-67-3
(1R,2S,3S,4S,6R)-2,6-dimethyl-4-(phenylsulfonyl)-4-(2-propenyl)-3-<3-((2-(trimethylsilyl)ethoxy)carbonyl)-2-oxopropyl>cyclohexane-1,2-diol 1,2-diacetonide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine / 1.) methylene chloride, 0 deg C, 1 h; 25 deg C, 1 h, 2.) benzene, reflux, 12 h

2: 1.) KDA / 1.) THF

With pyridine; Diethoxy-methyl-(6-amino-hexylaminomethyl)-silan;
DOI:10.1021/ja00385a030