3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

Base Information

Chemical Name:3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol
CAS No.:632293-73-3
Molecular Formula:C₆₈H₆₆O₁₀
Molecular Weight:1043.27
Hs Code.:

Synonyms:3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

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Chemical Property of 3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

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Technology Process of 3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

There total 7 articles about 3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 115-77-5
Pentaerythritol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 632293-73-3
3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

Guidance literature:: With pyridine; dmap; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 10h;

Reference yield: 70.0%

: 115-77-5
Pentaerythritol

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 632293-74-4
O-(4,4'-dimethoxytrityl)-pentaerythritol

: 532394-83-5
2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propane-1,3-diol

: 632293-73-3
3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

Guidance literature:: With pyridine; dmap;
DOI:10.1055/s-2003-41406

Reference yield:

: 19309-39-8
1-methyl-4-(hydroxymethyl)-2,6,7-trioxabicyclo-[2.2.2]-octane

: 632293-73-3
3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2,2-bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-propan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / dimethyl sulfoxide

2: hydrogenchloride / methanol

3: pyridine

4: hydrogen; palladium on activated charcoal

With pyridine; hydrogenchloride; palladium on activated charcoal; hydrogen; potassium hydroxide; In methanol; dimethyl sulfoxide;