N-<4-butyl>phthalimide

Base Information

Chemical Name:N-<4-butyl>phthalimide
CAS No.:86088-63-3
Molecular Formula:C₂₆H₂₆N₂O₆S₂
Molecular Weight:526.634
Hs Code.:

N-<4-<N,N-bis(p-toluenesulfonylamino)>butyl>phthalimide

Synonyms:N-<4-butyl>phthalimide

Suppliers and Price of N-<4-butyl>phthalimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-butyl>phthalimide

Chemical Property:

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Technology Process of N-<4-butyl>phthalimide

There total 5 articles about N-<4-butyl>phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 15544-49-7
N-(N⁴-p-toluenesulfonyl)-4-aminobutylphthalimide

: 98-59-9
p-toluenesulfonyl chloride

: 86088-63-3
N-<4-butyl>phthalimide

Guidance literature:: With sodium hydride; 1.) DMF, -50 deg C, 30 min, 2.) -50 deg C, 30 min;
DOI:10.1021/ja00354a047

Reference yield:

: 5460-29-7
2-(3-bromopropyl)isoindole-1,3-dione

: 86088-63-3
N-<4-butyl>phthalimide

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / dimethylsulfoxide / 2 h / 65 °C

2: 54.5 percent / H₂, HCl conc. / PtO₂ / ethanol / 24 h / 2327.2 Torr

3: 87.6 percent / Et₃N / CH₂Cl₂ / 4 h

4: 19 percent / 1.) NaH / 1.) DMF, -50 deg C, 30 min, 2.) -50 deg C, 30 min

With hydrogenchloride; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane; dimethyl sulfoxide;
DOI:10.1021/ja00354a047

Reference yield:

: 3184-61-0
4-phthalimidobutyronitrile

: 86088-63-3
N-<4-butyl>phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 54.5 percent / H₂, HCl conc. / PtO₂ / ethanol / 24 h / 2327.2 Torr

2: 87.6 percent / Et₃N / CH₂Cl₂ / 4 h

3: 19 percent / 1.) NaH / 1.) DMF, -50 deg C, 30 min, 2.) -50 deg C, 30 min

With hydrogenchloride; hydrogen; sodium hydride; triethylamine; platinum(IV) oxide; In ethanol; dichloromethane;
DOI:10.1021/ja00354a047