Technology Process of C18H26INO5
There total 4 articles about C18H26INO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C
1.2: 15 °C
2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C
3.1: iodine; silver sulfate / methanol
With
hydrogen; iodine; silver sulfate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 15 °C
1.2: 15 °C
2.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C
2.2: 15 °C
3.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C
4.1: iodine; silver sulfate / methanol
With
hydrogen; iodine; caesium carbonate; silver sulfate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide / 0.5 h / 15 °C
1.2: 15 °C
2.1: hydrogen / palladium on activated charcoal / methanol / 3 h / 15 °C
3.1: iodine; silver sulfate / methanol
With
hydrogen; iodine; silver sulfate; triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; palladium on activated charcoal;
In
methanol; N,N-dimethyl-formamide;