(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

Base Information

Chemical Name:(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide
CAS No.:170900-86-4
Molecular Formula:C₁₂H₁₇NO₂S
Molecular Weight:239.338
Hs Code.:

(+)-(R<sub>S</sub>)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ<sup>6</sup>,3]oxathiazole 2-oxide

Synonyms:(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

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Chemical Property of (+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

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Technology Process of (+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

There total 1 articles about (+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₈ClNO₂S

: 170900-86-4
(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at -78 ℃; for 0.25h; Yield given;
DOI:10.1016/00404-0399(50)1195N-

Reference yield:

: 170900-86-4
(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

: C₁₃H₂₁NO₂S

Guidance literature:: (+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide; With methyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 0.833333h;

With water; ammonium chloride; In tetrahydrofuran; hexane;

Reference yield:

: 4784-77-4,29576-14-5,39616-19-8
(E/Z)-crotyl bromide

: 170900-86-4
(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide

: (R_S,1R)-N-[1-(hydroxymethyl)-2-methylpropyl]-S-(2-butenyl)-p-toluenesulfoximide

Guidance literature:: (E/Z)-crotyl bromide; With magnesium; In diethyl ether; at 0 ℃; Heating / reflux;

With 1,10-Phenanthroline; (-)-menthol; In tetrahydrofuran; diethyl ether;

(+)-(R_S)-4(R)-isopropyl-2-p-tolyl-4,5-dihydro[1,2λ⁶,3]oxathiazole 2-oxide; With water; ammonium chloride; more than 3 stages;