(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

Base Information

Chemical Name:(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide
CAS No.:1011243-18-7
Molecular Formula:C₂₄H₄₃NO₅Si
Molecular Weight:453.695
Hs Code.:

Synonyms:(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

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Technology Process of (2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

There total 1 articles about (2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 779338-03-3
C₁₈H₂₉NO₅

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1011243-18-7
(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/jo7024515

Reference yield: 97.0%

: 1011243-18-7
(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide

: 756-79-6
dimethyl methane phosphonate

: 1011243-02-9
dimethyl (3R,4S)-4-(4-methoxybenzyloxy)-3-methyl-2-oxo-8-(triethylsilyloxy)octylphosphonate

Guidance literature:: dimethyl methane phosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.25h;

(2R,3S)-N-methoxy-3-(4-methoxybenzyloxy)-N,2-dimethyl-7-(triethylsiloxy)heptanamide; In tetrahydrofuran; hexane; at -78 - 0 ℃; Further stages.;
DOI:10.1021/jo7024515