4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Base Information

Chemical Name:4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
CAS No.:1172615-43-8
Molecular Formula:C₂₁H₁₃F₉N₂O₃S
Molecular Weight:544.397
Hs Code.:

Synonyms:4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Chemical Property of 4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Technology Process of 4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

There total 1 articles about 4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 375-72-4
Nonafluorobutanesulfonyl fluoride

: 1172615-42-7
4-methyl-2,6-diphenylpyrimidin-5-ol

: 1172615-43-8
4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: 4-methyl-2,6-diphenylpyrimidin-5-ol; With sodium hydride; In tetrahydrofuran; for 0.0833333h;

Nonafluorobutanesulfonyl fluoride; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1055/s-0028-1088220

Reference yield: 73.0%

: 1172615-43-8
4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 536-74-3
phenylacetylene

: 1172615-44-9
4-methyl-2,6-diphenyl-5-(phenylethynyl)pyrimidine

Guidance literature:: With copper(l) iodide; palladium diacetate; diisopropylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 70 ℃; for 3h;
DOI:10.1055/s-0028-1088220

Reference yield: 47.0%

: 1172615-43-8
4-methyl-2,6-diphenylpyrimidin-5-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 6783-05-7
trans-2-phenylvinylboronic acid

: 1229662-07-0
(E)-4-methyl-2,6-diphenyl-5-styrylpyrimidine

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; at 70 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201000056