cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

Base Information

Chemical Name:cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)
CAS No.:111848-64-7
Molecular Formula:C₃₅H₅₉ClP₂Pt
Molecular Weight:772.334
Hs Code.:

Synonyms:cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

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Chemical Property of cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

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Technology Process of cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

There total 1 articles about cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 111848-63-6
cis-chloro(3,5-dimethylbenzyl)(1,5-cyclooctadiene)platinum(II)

: 23743-26-2
1,2-bis-(dicyclohexylphosphino)ethane

: 111848-64-7
cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

Guidance literature:: In dichloromethane; addn. of bis(dicyclohexylphosphino)ethane to cis-chloro(3,5-dimethylbenzyl)(1,5-cyclooctadiene)platinum(II) in CH2Cl2 under Ar at room temp., after 2 h solvent evapn.; recrystn. from acetone, crystn. at -10°C, suction filtration;
DOI:10.1021/ja00213a016

Reference yield: 34.0%

: 111848-64-7
cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

: 105373-24-8
cis-hydrido(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II)

Guidance literature:: With Na{HB(OMe)3}; In tetrahydrofuran; treating cis-chloro(3,5-dimethylbenzyl){bis(dicyclohexylphosphino)ethane}platinum(II) with NaHB(OMe)3 in THF became cloudy, after 1 h at room temp. quenched by H2O at 0°C; ether added, org. layer sepd., aq. layer extd. with ether, evapd., resulting oil dissolved in minimum THF, 1 part MeOH added, crystn. at -10°C, once recrystd., suction filtrn.;
DOI:10.1021/ja00213a016