3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

Base Information

Chemical Name:3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate
CAS No.:1223615-76-6
Molecular Formula:C₃₉H₆₃N₃O₁₁
Molecular Weight:749.943
Hs Code.:

Synonyms:3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

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Chemical Property of 3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

Chemical Property:

Purity/Quality:

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Technology Process of 3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

There total 4 articles about 3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₁H₆₅N₃O₁₂

: 1223615-76-6
3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

Guidance literature:: With methanol; at 55 ℃; for 20h;
DOI:10.1016/j.ejmech.2009.11.032

Reference yield:

: 1223615-38-0
C₃₇H₆₀N₄O₁₂

: 1223615-76-6
3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine hydrochloride / 20 °C

2: methanol / 12 h / Heating

With pyridine hydrochloride; In methanol;
DOI:10.1016/j.ejmech.2016.10.065

Reference yield:

: 83905-01-5,92470-27-4
Zithromax(R)

: 1223615-76-6
3-O-(benzyl)-N-methylcarbamoyl descladinosylazithromycin-11,12-cyclic carbonate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / ethanol; water / 20 h / 20 °C

2: triethylamine / dichloromethane / 24 h / 20 °C

3: triethylamine / toluene / 72 h / 55 °C

4: pyridine hydrochloride / 20 °C

5: methanol / 12 h / Heating

With hydrogenchloride; pyridine hydrochloride; triethylamine; In methanol; ethanol; dichloromethane; water; toluene;
DOI:10.1016/j.ejmech.2016.10.065