Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester

Base Information

• Chemical Name: Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester
• CAS No.: 144181-07-7
• Molecular Formula: C₄₂H₃₆Br₆O₁₂
• Molecular Weight: 1212.16
• Mol file: 144181-07-7.mol

Synonyms:Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester

Chemical Property of Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester

There total 1 articles about Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-benzene tris(carbonyl chloride) (4422-95-1) + tert-butyl 3,5-dibromosalicylate (88797-22-2) → Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester (144181-07-7)

Guidance literature:

With potassium tert-butylate; Yield given. Multistep reaction; 1.) THF, RT, 15 min, 2.) THF, RT, overnight;

DOI:10.1021/ja00050a005

Reference yield: 82.0%

Benzene-1,3,5-tricarboxylic acid tris-(2,4-dibromo-6-tert-butoxycarbonyl-phenyl) ester (144181-07-7) → trimesoyl tris(3,5-dibromosalicylate) (144181-06-6)

Guidance literature:

With trifluoroacetic acid; for 1h; Ambient temperature;

DOI:10.1021/ja00050a005

upstream raw materials:

1,3,5-benzene tris(carbonyl chloride)

tert-butyl 3,5-dibromosalicylate

Downstream raw materials:

trimesoyl tris(3,5-dibromosalicylate)