C₂₄H₃₂Cl₂N₆O₂

Base Information

• Chemical Name: C₂₄H₃₂Cl₂N₆O₂
• CAS No.: 906806-16-4
• Molecular Formula: C₂₄H₃₂Cl₂N₆O₂
• Molecular Weight: 507.463
• Mol file: 906806-16-4.mol

Synonyms:C₂₄H₃₂Cl₂N₆O₂

Chemical Property of C₂₄H₃₂Cl₂N₆O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₂Cl₂N₆O₂

There total 6 articles about C₂₄H₃₂Cl₂N₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H35ClN6O4 (907181-40-2) → C24H32Cl2N6O2 (906806-16-4)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 20 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2011.09.120

Reference yield:

(S)(+)-2-ethylpiperazine (207284-20-6) → C24H32Cl2N6O2 (906806-16-4)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium diacetate; caesium carbonate / 1,4-dioxane / 90 °C

2: titanium(IV) isopropylate; sodium cyanoborohydride / 1,2-dichloro-ethane / 60 °C

3: trifluoroacetic acid / dichloromethane / 20 °C

4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

With titanium(IV) isopropylate; palladium diacetate; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; caesium carbonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2011.09.120

Reference yield:

methyl 6-amino-2,3-dichloropyrazine-5-carboxylate (1458-18-0) → C24H32Cl2N6O2 (906806-16-4)

Guidance literature:

Multi-step reaction with 4 steps

1: palladium diacetate; caesium carbonate / 1,4-dioxane / 90 °C

2: titanium(IV) isopropylate; sodium cyanoborohydride / 1,2-dichloro-ethane / 60 °C

3: trifluoroacetic acid / dichloromethane / 20 °C

4: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane

With titanium(IV) isopropylate; palladium diacetate; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; caesium carbonate; trifluoroacetic acid; In 1,4-dioxane; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1016/j.bmcl.2011.09.120

upstream raw materials:

C₁₂H₁₈ClN₅O₂

C₁₇H₂₇ClN₆O₂

4-chlorobenzaldehyde

C₂₂H₃₅ClN₆O₄

Downstream raw materials:

C₂₅H₃₅Cl₂N₇O

C₂₃H₃₂Cl₂N₈O