Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester

Base Information

• Chemical Name: Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester
• CAS No.: 103174-93-2
• Molecular Formula: C₁₉H₁₇NO₂S
• Molecular Weight: 323.415
• Mol file: 103174-93-2.mol

Synonyms:Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester

Chemical Property of Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester

There total 1 articles about Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

acetic anhydride (108-24-7) + C17H15NOS (78839-90-4) → Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester (103174-93-2)

Guidance literature:

for 5h; Heating;

DOI:10.1055/s-1988-27475

Reference yield: 26.0%

Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester (103174-93-2) → 10a-acetyl-10a,11-dihydrobenzindeno<1,2-e><1,4>thiazine + 4-<2-(benzothiazol-2-yl)phenyl>-butan-2-one (78840-25-2) + 5-acetyl-5,11-dihydrobenzindeno<1,2-e><1,4>thiazine

Guidance literature:

In dimethyl sulfoxide; for 5h; Heating;

Reference yield:

Thioacetic acid S-{2-[acetyl-(3H-inden-1-yl)-amino]-phenyl} ester (103174-93-2) → thioacetic acid S-(2-acetylamino-phenyl)ester (1204-55-3) + inden-1-one (83-33-0)

Guidance literature:

With hydrogenchloride; In chloroform; at 50 ℃; for 1h;

DOI:10.1055/s-1988-27475

upstream raw materials:

acetic anhydride

C₁₇H₁₅NOS

Downstream raw materials:

thioacetic acid S-(2-acetylamino-phenyl)ester

inden-1-one

4-<2-(benzothiazol-2-yl)phenyl>-butan-2-one