N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

Base Information

Chemical Name:N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid
CAS No.:1586819-49-9
Molecular Formula:C₃₁H₂₄Cl₄N₂O₆
Molecular Weight:662.353
Hs Code.:

Synonyms:N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

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Chemical Property of N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

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Technology Process of N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

There total 4 articles about N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1586819-33-1
N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

: 1586819-49-9
N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1134/S1070428014020122

Reference yield:

: 1586819-23-9
N-[4-(4-amino-2-methoxybenzyl)-2-methoxyphenyl]imide of endo,exo-1,2,3,4,11,11-hexachlorotricyclo[6.2.1.0^5,10]undec-2-ene-7,8-dicarboxylic acid

: 1586819-49-9
N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 6 h / 150 °C

2: pyridine / N,N-dimethyl-formamide / 20 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1134/S1070428014020122

Reference yield:

: 4,4'-methylene-bis[3-methoxy]benzenamine

: 1586819-49-9
N-{4-[4-(maleimido)-2-methoxybenzyl]-2-methoxyphenyl}imide of endo,exo-2,3,4,5-tetrachlorobicyclo[4.4.0]deca-2,4-diene-8,9-dicarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 6 h / 150 °C

2: N,N-dimethyl-formamide / 6 h / 150 °C

3: pyridine / N,N-dimethyl-formamide / 20 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1134/S1070428014020122