C₃₈H₆₁NO₇SSi₂

Base Information

Chemical Name:C₃₈H₆₁NO₇SSi₂
CAS No.:1622094-39-6
Molecular Formula:C₃₈H₆₁NO₇SSi₂
Molecular Weight:732.142
Hs Code.:

C<sub>38</sub>H<sub>61</sub>NO<sub>7</sub>SSi<sub>2</sub>

Synonyms:C₃₈H₆₁NO₇SSi₂

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Chemical Property of C₃₈H₆₁NO₇SSi₂

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Technology Process of C₃₈H₆₁NO₇SSi₂

There total 18 articles about C₃₈H₆₁NO₇SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1622094-31-8
C₄₀H₆₁NO₉SSi₂

: 1622094-39-6
C₃₈H₆₁NO₇SSi₂

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201402323

Reference yield:

: 1622094-28-3
C₄₀H₅₉NO₈SSi₂

: 1622094-39-6
C₃₈H₆₁NO₇SSi₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

2.1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: lithium iodide monohydrate / ethyl acetate / 8 h / 20 °C / Reflux

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.1: iodine; [bis(acetoxy)iodo]benzene / dichloromethane / 2 h / 20 °C / Inert atmosphere

5.2: 0.5 h

6.1: diisobutylaluminium hydride / toluene / 20 h / 20 °C / Inert atmosphere

With dmap; lithium borohydride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; diisobutylaluminium hydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene;
DOI:10.1002/chem.201402323

Reference yield:

: 179260-96-9
4-methoxy-3-(triisopropylsilyloxy)-benzaldehyde

: 1622094-39-6
C₃₈H₆₁NO₇SSi₂

Guidance literature:: Multi-step reaction with 16 steps

1.1: silver nitrate; iodine / dichloromethane / 14 h / 20 °C / Inert atmosphere

2.1: copper dichloride; tert.-butylhydroperoxide / acetonitrile; water / 16 h / 20 - 50 °C

3.1: thionyl chloride / dichloromethane / 2 h / 20 °C / Inert atmosphere; Reflux

4.1: water; tetrahydrofuran / 0.08 h

4.2: 2 h / 0 °C

5.1: lithium iodide monohydrate / ethyl acetate / 48 h / 20 °C / Reflux

6.1: [bis(acetoxy)iodo]benzene / dichloromethane / 0.17 h / 20 °C

7.1: potassium hydroxide / water; methanol / 0.25 h / -20 °C

8.1: 2,6-dimethylpyridine / dichloromethane / 3 h / 20 °C / Inert atmosphere

9.1: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / acetonitrile; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.1: triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

11.1: lithium borohydride / tetrahydrofuran / 6 h / -78 °C / Inert atmosphere

12.1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

13.1: lithium iodide monohydrate / ethyl acetate / 8 h / 20 °C / Reflux

14.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere

15.1: iodine; [bis(acetoxy)iodo]benzene / dichloromethane / 2 h / 20 °C / Inert atmosphere

15.2: 0.5 h

16.1: diisobutylaluminium hydride / toluene / 20 h / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; tert.-butylhydroperoxide; dmap; lithium borohydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; lithium iodide monohydrate; [bis(acetoxy)iodo]benzene; iodine; diisobutylaluminium hydride; silver nitrate; triethylamine; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; toluene; acetonitrile; 4.1: |Schotten-Baumann Reaction;
DOI:10.1002/chem.201402323